24(3) |
L13 |
ZORBAX TMS |
Assay |
|
32(3) |
L13 |
Adsorbosphere TMS |
Assay |
4.6 mm x 25 cm, 5 µm. |
24(3) |
L7 |
Symmetry C8 |
Chromatographic purity |
5-µm |
0(0) |
L7 |
ZORBAX SB C8 |
Chromatographic purity |
Test 1. Alternative column Symmetry C8 (Waters). |
0(0) |
L1 |
Luna C18 |
Chromatographic purity |
Test 2. 15 cm x 4.6 mm, 5 µm. |
29(1) |
L51 |
Chiralpak AD |
Limit of . . . . . . . . . |
Limit of related compound C. 25 cm x 4.6 mm. |
31(1) |
L1 |
Purospher STAR RP18e |
Limit of . . . . . . . . . |
Limit of 1-methyl-4-(p-fluorophenyl)-1,2,3,6-tetrahydropyridine. 4.0 mm x 25 cm. |
24(3) |
L1 |
Hypersil BDS C-18 |
Limit of . . . . . . . . . |
Limit of 1-methyl-4-(p-fluorophenyl)-1,2,3,6-tetrahydropyridine. |
24(3) |
L13 |
ZORBAX TMS |
Limit of . . . . . . . . . |
Limit of related compound D. |
24(3) |
G43 |
None Cited |
Organic volatile impurities |
See Method V 467 |